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Preparation of glass-ceramics using gasification residue of sewage sludge

机译:利用污泥气化残渣制备微晶玻璃

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Glass-ceramic was successfully prepared by mixing limestone, dolomite, Cr2O3 and TiO2 with gasification residue of sewage sludge. The parent glass melted at 1450°C for 2 h can be bulk crystallized by twostep heat-treatment, i.e., nucleation at 750°C for 1 h and crystallization at 1000°C for 1.5 h. The main crystal phase of the glass-ceramics consists of angite as determined by XRD and presents interlocking structure of prismatic crystals under ESEM. Results of leaching experiments (TCLP test) show that heavy metals from the sewage sludge were solidified in the glass-ceramics. Therefore the proposed approach of sewage sludge residue recycling proves to be economically and environmentally viable.
机译:将石灰石,白云石,Cr2O3和TiO2与污水污泥的气化残余物混合,成功制备了微晶玻璃。可以通过两步热处理,即在750℃下成核1小时并在1000℃下结晶1.5小时,使在1450℃下熔融2小时的母玻璃体结晶。玻璃陶瓷的主晶相由X射线衍射确定的方铁矿组成,并且在ESEM下呈现棱柱晶体的互锁结构。浸出实验(TCLP测试)的结果表明,污水污泥中的重金属在玻璃陶瓷中固化。因此,所提出的污水污泥残渣循环利用方法被证明在经济和环境上都是可行的。

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