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Gas sensing properties of nanocrystalline metal oxide powders prepared by sol-gel method

机译:溶胶-凝胶法制备的纳米晶金属氧化物粉末的气敏特性

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SnO2 nonopowders were prepared by sol-gel method and exposed to different thermal decomposition. The XRD and TEM analysis have been carried out. At higher temperature X-ray diffraction peaks are sharper with more intensified peaks. AlsoTEM micrograph reveals that the grain size of nanopowders changed from 10 nm to 80 nm regarding to different thermal treatment. The gas response shows characteristic dependence on dm (grain size). Responses to H2 and LPG gas as a function of operation temperature in dry air for the analyzed sensors with different nano powders show that smaller grain size are more sensitive to H2 and LPG gas.
机译:通过溶胶-凝胶法制备了SnO2非粉末,并经受了不同的热分解。进行了XRD和TEM分析。在更高的温度下,X射线衍射峰更加尖锐,而峰强度更大。另外TEM显微照片显示,关于不同的热处理,纳米粉末的晶粒尺寸从10nm改变为80nm。气体响应显示出对dm(粒度)的特征依赖性。对于具有不同纳米粉末的分析传感器,H2和LPG气体随干燥空气中的工作温度变化的响应表明,较小的颗粒尺寸对H2和LPG气体更敏感。

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