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LUBE OIL PRODUCTION BY COMBINATION OF HYDROCONVERSION AND SOLVENT DEWAXING

机译:加氢转化和溶剂脱蜡相结合生产润滑油

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Due to insufficient capabilities for the solvent extraction in the Czech Republic, a technology for lube base oil production, comprising HP hydrocracking on existing equipment (originally designed for brown coal tar processing) and solvent dewaxing has been developed since the late fifties, resulting in the manufacture of high quality products. High flexibility in the lube oil components viscosity has been achieved by the development of a special catalyst and by using five types of vacuum gas oils of different viscosities as feedstocks. In order to maximise the utilization of the liquid products from a Hydrocracking unit for lube oil production and, furthermore, to widen the viscosity range, a unique vacuum distillation of the products has been developed, which makes it possible to withdraw five side cuts with viscosities in the range from 2 to 20 mm~2/s at 40 °C. The cuts with viscosities up to 15 mm~2/s at 40 °C have good low temperature properties without dewaxing. The cuts and residues with higher viscosities have to be dewaxed by a MEK-toluene mixture, yielding different grades of refined paraffin waxes as by-products.The stability of hydrocracked oils are considerably influenced by the remaining polyaromatics content, which depends on the feed quality and hydrocracking unit operating parameters. Desired properties of the resulting base lube oil components, including their oxidation stability, are achieved both by their manufacturing on three levels of viscosity index (95, 105, 130) and by mixing them with components manufactured by the selective extraction.
机译:由于捷克共和国的溶剂萃取能力不足,自五十年代末期以来,已开发出一种润滑油基础油生产技术,包括在现有设备上进行HP加氢裂化(最初设计用于褐煤焦油加工)和溶剂脱蜡。制造高品质的产品。通过开发一种特殊的催化剂并通过使用五种不同粘度的真空瓦斯油作为原料,可以实现润滑油组分粘度的高柔韧性。为了最大程度地利用加氢裂化装置中的液体产品来生产润滑油,并且为了扩大粘度范围,已经开发了一种独特的产品真空蒸馏技术,可以抽出五个粘度高的侧馏分在40°C下为2至20 mm〜2 / s的范围内。在40°C时粘度最高为15 mm〜2 / s的切口具有良好的低温性能,而不会脱蜡。具有较高粘度的切口和残留物必须通过MEK-甲苯混合物脱蜡,产生不同等级的精制石蜡作为副产品。 加氢裂化油的稳定性受剩余的多环芳烃含量的影响很大,这取决于进料质量和加氢裂化装置的运行参数。通过在三种水平的粘度指数(95、105、130)上进行制造并将其与通过选择性萃取制得的组分混合,可以实现所需基础润滑油组分的所需性能,包括其氧化稳定性。

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