首页> 外文会议>Materials science and technology conference;MSamp;T08; 20081005-09;20081005-09; Pittsburgh, PA(US);Pittsburgh, PA(US) >PREPARATION OF METAL OXIDE PHOTOCATALYST BY SOFT SOLUTION PROCESS WITH ANION EXCHANGE RESIN
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PREPARATION OF METAL OXIDE PHOTOCATALYST BY SOFT SOLUTION PROCESS WITH ANION EXCHANGE RESIN

机译:阴离子交换树脂软溶液法制备金属氧化物光催化剂

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摘要

Photocatalysts are expected for removing an environmental pollutant only with solar energy. Generally, the photocatalic powders are synthesized with high energy process such as the solid-phase synthesis or gas-phase process. On the other hand, there is a concept for making high performance material directly from solution, in soft and environmentally friendly condition, which is called soft solution process. In this study, zinc hydroxide and oxide were synthesized by ion exchange resin. By this method, we succeeded in harmless and energy saving process. Afterwards, the basic physical properties and photocatalic performance of the obtained sample were evaluated. The as-prepared photocatalyst was characterized by TG-DTA, XRD, FE-SEM, BET, and UV-vis and ZnO calcined at 573 K showed the highest photocatalic activity.
机译:期望光催化剂仅利用太阳能去除环境污染物。通常,光催化粉末是通过诸如固相合成或气相法的高能方法合成的。另一方面,存在一种在柔软且环境友好的条件下直接从溶液中制备高性能材料的概念,称为柔软溶液法。在这项研究中,氢氧化锌和氧化物是通过离子交换树脂合成的。通过这种方法,我们成功实现了无害且节能的过程。然后,评估所获得样品的基本物理性质和光催化性能。所制备的光催化剂通过TG-DTA,XRD,FE-SEM,BET和UV-vis表征,在573 K下煅烧的ZnO表现出最高的光催化活性。

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