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Synthesis of Tungsten Carbide from Bacterial Cellulose

机译:由细菌纤维素合成碳化钨

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Here we present preliminary experiments for the synthesis of carbide material using bacterial cellulose as carbon source. We used bacteria cellulose available as Nata de Coco and infiltrated it with tungsten trioxide (WO_3) nanoparticles. This composite was heat treated at 1300 ℃ in nitrogen atmosphere. The XRD pattern confirms the synthesis of tungsten carbide (WC) in the carbonaceous material, though a significant amount of metallic tungsten remained unreacted. SEM images shows that WC particles are present only at the surface of the carbon, which may be a consequence of improper infiltration or collapse of carbon matrix during heat treatment.
机译:在这里,我们介绍了使用细菌纤维素作为碳源合成碳化物材料的初步实验。我们使用了可得的Nata de Coco细菌纤维素,并用三氧化钨(WO_3)纳米颗粒渗透了它。将该复合材料在氮气气氛中于1300℃进行热处理。 XRD图谱证实了含碳材料中碳化钨(WC)的合成,尽管仍有大量未反应的金属钨。 SEM图像表明,WC颗粒仅存在于碳的表面,这可能是热处理过程中碳基体渗透或塌陷的结果。

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