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Characteristics of FeCuAl Powder Compacts Formed through Uniaxial Die Compaction Route

机译:单轴压模成型的FeCuAl粉末压块的特性

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摘要

This paper presents the development of FeCuAl powder compacts through uniaxial die compaction process. Iron powder ASC 100.29 was mechanically mixed with other elemental powders, i.e., copper (Cu), and aluminum (Al) for 30 minutes at a rotation of 30 rpm. The feedstock was subsequently shaped at three different temperatures, i.e., 30℃, 150℃, and 200℃ through simultaneous upward and downward axial loading of 325 MPa. The as-pressed samples termed as green compacts were then sintered in argon gas fired furnace at 800℃ for three different holding times, i.e., 30,60, and 90 min at a rate of 10℃/min. The sintered samples were characterized for their relative density, electrical resistivity, and bending strength. The microstructure of the sintered samples was also evaluated through scanning electron microscopy (SEM). The results revealed that the sample formed at 150℃ and sintered for 30 min obtained the best final characteristics, i.e., higher relative density, lower volumetric expansion and electrical resistivity, and higher bending strength. Microstructure evaluation also revealed that the sample formed at 150℃ and sintered for 30 min obtained more homogeneous distribution of grains and less interconnected pores compared to the other samples.
机译:本文介绍了通过单轴压模工艺制备FeCuAl粉末压块的方法。将铁粉ASC 100.29与其他元素粉(即铜(Cu)和铝(Al))以30 rpm的转速机械混合30分钟。随后,通过同时施加向上和向下的轴向轴向载荷325 MPa,使原料在三个不同的温度(即30℃,150℃和200℃)下成型。然后将压制的称为生坯的样品在800℃的氩气燃烧炉中以10℃/ min的速率烧结三个不同的保温时间,即30,60和90分钟。对烧结样品的相对密度,电阻率和弯曲强度进行表征。还通过扫描电子显微镜(SEM)评估了烧结样品的微观结构。结果表明,在150℃下成型并烧结30分钟的样品具有最佳的最终特性,即较高的相对密度,较低的体积膨胀率和电阻率以及较高的弯曲强度。显微组织评估还显示,与其他样品相比,在150℃下成型并烧结30分钟的样品获得了更均匀的晶粒分布和更少的互连孔。

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  • 来源
  • 会议地点 Bangi(MY)
  • 作者单位

    Centre for Advanced Materials, College of Engineering, Universiti Tenaga Nasional, Putrajaya Campus, 43000 Kajang, Selangor, Malaysia;

    Centre for Advanced Materials, College of Engineering, Universiti Tenaga Nasional, Putrajaya Campus, 43000 Kajang, Selangor, Malaysia;

    Centre for Advanced Materials, College of Engineering, Universiti Tenaga Nasional, Putrajaya Campus, 43000 Kajang, Selangor, Malaysia;

  • 会议组织
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    Uniaxial die compaction; forming temperature; sintering time; microstructure;

    机译:单轴压模;成型温度烧结时间微观结构;

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