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Preparation and characterization of conductive antimony-doped tin oxide (ATO) nanoparticles

机译:导电锑掺杂氧化锡(ATO)纳米粒子的制备与表征

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In this paper, conductive antimony-doped tin oxide (ATO) composite particles is prepared by hydroxylation method of metal alcoxides. This method has many advantages such as little pollution, low-cost , simple sheet and equipment. The synthesis processing and the ATO nanoparticles are characterized by means of transmission electron microscope (TEM), X-ray diffraction (XRD), thermal gravimetric and differential thermal analysis, and BET. The results show that the ATO nanoparticles is tetragonal rutile crystal structure. TEM show that the particles are monodispersed with weak aggromation. The size of the particles calcinated at 700 is about 8nm. The specific areas are 153 m~2·g~(-1). In addition to, ATO nanoparticles have good electric properties.
机译:本文采用羟基氧化金属铝氧化物的方法制备了导电锑掺杂氧化锡(ATO)复合颗粒。该方法具有污染少,成本低,板材和设备简单等优点。借助透射电子显微镜(TEM),X射线衍射(XRD),热重分析和差热分析以及BET对合成过程和ATO纳米颗粒进行表征。结果表明,ATO纳米颗粒为四方金红石型晶体结构。 TEM显示颗粒是单分散的,具有弱的团聚作用。在700℃煅烧的颗粒的尺寸为约8nm。比面积为153 m〜2·g〜(-1)。此外,ATO纳米粒子具有良好的电性能。

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