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Research on Micro-Mechanism of Nano-Composite Ceramic in Two-Dimensional Ultrasound Grinding

机译:纳米复合陶瓷二维超声磨削的微观机理研究

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Surface microstructure of nano-composite ceramics prepared by mixed coherence system and machined by two-dimensional ultrasonic precision grinding was researched using TEM, SEM, XRD detector and other equipments. Structure, formation mechanism and characteristic of metamorphic layer of ground surface of nano-composite ceramics were researched. The experiment shows micro deformation mechanism of ceramic material in two-dimensional ultrasound grinding is twin grain boundary and grain-boundary sliding for A1<,2>O<,3>, and it is crystal dislocation of enhanced phase, matrix grain boundary sliding, coordination deformation of intergranular second phase as well as its deformation mechanism for nano-composite ceramics. The fracture surfaces of nano-composite materials with different microscopic structure were observed using TEM and SEM. Research shows that ZrO<,2> plays an important influence on the generation and expansion of crack, and enhances the strength of grain boundaries. When grain boundaries is rich in the ZrO<,2> particles, the crack produced in grinding process will be prevented, and the surface with plastic deformation will be smooth. The results shows nanoparticles dispersed in grain boundary prevents crack propagation and makes materials fracture transgranularly which makes the processed surface fine.
机译:利用TEM,SEM,XRD检测仪等设备研究了混合相干体系制备的二维超声精密磨削加工的纳米复合陶瓷的表面微观结构。研究了纳米复合陶瓷基表面变质层的结构,形成机理和特性。实验表明,二维超声磨削中陶瓷材料的微观形变机理为A1,2O <,3>为双晶界和晶界滑动,增强相的晶体位错,基体晶界滑动,纳米复合陶瓷晶间第二相的配位变形及其变形机理使用TEM和SEM观察了具有不同微观结构的纳米复合材料的断裂表面。研究表明,ZrO <,2>对裂纹的产生和扩展具有重要影响,并增强了晶界的强度。当晶界中富含ZrO,2颗粒时,将防止在研磨过程中产生裂纹,并且具有塑性变形的表面将变得光滑。结果表明,分散在晶界中的纳米颗粒可防止裂纹扩展,并使材料跨晶断裂,从而使加工表面细化。

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