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Investigation of Magnetic Properties of Co0.2Zn0.8Fe2O4Nanoparticles for Hyperthermia Applications

机译:用于热疗的Co 0.2 Zn 0.8 Fe 2 O 4 纳米粒子的磁性研究

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Con0.2nZnn0.8nFen2nOn4nnanoparticles were prepared by high temperature thermal decomposition method [1]. The crystal structure, measured by x-ray diffraction, was cubic spinel with space group Fd-3m and the lattice constant (ao) of 8.4051 Å from Rietveld refinement analysis. Based on the Scherrer equation, the average diameter of nanoparticles was estimated to be 13.4 nm. The magnetic properties were investigated using a vibrating sample magnetometer and 57Fe Mössbauer spectroscopy. The values of saturation magnetization and coercivity of COon0.2nZnn0.8nFen2nOn4nnanoparticles at room temperature were 86.75 emu/g and 31.66 Oe, respectively. The thermal properties for hyperthermia applications were measured by magneTherm device within physiologically safe ranges of frequency and amplitude. The self-heating temperature was estimated to be 123 and 129 °C at 50 and 112 kHz under 25 mT, respectively.
机译:Con 0.2 nZnn 0.8 nFen < inf xmlns:mml =“ http://www.w3.org/1998/Math/MathML” xmlns:xlink =“ http://www.w3.org/1999/xlink”> 2 nOn 4 nnanoparticles的制备方法如下:高温热分解法[1]。通过X射线衍射测量的晶体结构为立方尖晶石,其空间群为Fd-3m,根据Rietveld细化分析,其晶格常数(ao)为8.4051Å。基于Scherrer方程,纳米粒子的平均直径估计为13.4 nm。使用振动样品磁力计和57FeMössbauer光谱仪研究了磁性。 COon 0.2 nZnn 0.8 nFen 2 nOn 4室温下的纳米颗粒分别为86.75 emu / g和31.66 Oe。通过magneTherm装置在生理和频率安全范围内测量热疗的热性能。在25 mT下,自加热温度在50 kHz和112 kHz时分别估计为123和129°C。

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