首页> 外国专利> Chitosan-Gelatin Hydrogels for heavy metal adsorption and chitosan-gelatin hydrogels manufactured by the same method

Chitosan-Gelatin Hydrogels for heavy metal adsorption and chitosan-gelatin hydrogels manufactured by the same method

机译:用相同方法制造的重金属吸附和壳聚糖 - 明胶水凝胶的壳聚糖 - 明胶水凝胶

摘要

The present invention uses a crosslinking agent to crosslink chitosan and gelatin to efficiently remove heavy metals harmful to the human body, such as lead, cadmium, mercury, and chromium, in contaminated wastewater, and a method for manufacturing a chitosan-gelatin hydrogel for adsorption of heavy metals. It relates to a hydrogel prepared according to the The present invention is a first step of preparing a chitosan solution by adding chitosan having a weight average molecular weight of 100,000 to 200,000 to an acidic aqueous solution, and dispersing it at room temperature for 1 to 24 hours; a second step of preparing a gelatin solution by adding gelatin having a weight average molecular weight of 100,000 to 200,000 to water and dispersing it at a temperature of 20 to 50° C. for 1 to 5 hours; A third step of mixing the chitosan solution and the gelatin solution; a fourth step of crosslinking the chitosan and gelatin by adding a crosslinking agent to the mixed solution; After the fourth step, a fifth step of preparing a hydrogel by separating and pulverizing the cross-linked chitosan-gelatin complex from the mixed solution; and a sixth step of washing so that the pH of the hydrogel is 6 to 7.5, and freeze-drying for 24 to 72 hours to solidify;
机译:本发明使用交联剂与交联壳聚糖和明胶有效地去除对人体有害的重金属,例如铅,镉,汞和铬,污染的废水,以及制造壳聚糖 - 明胶水凝胶的方法进行吸附重金属。它涉及根据本发明制备的水凝胶是通过将壳聚糖加入100,000至200,000至酸性水溶液中的壳聚糖制备壳聚糖溶液的第一步骤,并将其在室温下分散1至24小时;通过将重均分子量为100,000至200,000的凝胶素加入到水中并在20至50℃的温度下将其分散1至5小时,制备明胶溶液的第二步骤。混合壳聚糖溶液和明胶溶液的第三步;通过向混合溶液中添加交联剂来交联壳聚糖和明胶的第四步;在第四步之后,通过将交联的壳聚糖 - 明胶复合物与混合溶液分离和粉碎,制备水凝胶的第五步;和洗涤的第六步,使水凝胶的pH为6至7.5,并冷冻干燥24至72小时以固化;

著录项

  • 公开/公告号KR102351290B1

    专利类型

  • 公开/公告日2022-01-13

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR1020170114720

  • 发明设计人 정인우;론 싸이풀라;

    申请日2017-09-07

  • 分类号B01J20/24;B01J20/30;C02F1/28;

  • 国家 KR

  • 入库时间 2022-08-24 23:27:21

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