首页> 外国专利> METHOD FOR PRODUCING HIGH-PURITY BIS(2-HYDROXYETHYL) TEREPHTHALATE, REGENERATED POLY(ETHYLENE TEREPHTHALATE), DECOLORING SOLVENT, AND METHOD FOR PURIFYING BIS(2-HYDROXYETHYL) TEREPHTHALATE

METHOD FOR PRODUCING HIGH-PURITY BIS(2-HYDROXYETHYL) TEREPHTHALATE, REGENERATED POLY(ETHYLENE TEREPHTHALATE), DECOLORING SOLVENT, AND METHOD FOR PURIFYING BIS(2-HYDROXYETHYL) TEREPHTHALATE

机译:生产高纯度双(2-羟乙基)对苯二甲酸酯,再生聚(乙二醇酯),脱色溶剂和纯化双苯二甲酸酯的方法

摘要

[Problem] To provide a method for producing high-purity bis(2-hydroxyethyl) terephthalate (BHET), by which high-purity BHET can be easily produced from colored polyester waste. [Solution] A method for producing high-purity BHET according to the present invention comprises: a depolymerization step in which colored polyester waste is depolymerized to obtain a depolymerization product including colored crude BHET; a concentration step in which low-boiling ingredients contained in the depolymerization product are removed to concentrate the BHET; a recovery step in which the BHET is recovered from the crude BHET to obtain medium-purity BHET; a crystallization separation step in which the medium-purity BHET is subjected to crystallization in a decoloring solvent and the crystals are separated, by solid-liquid separation, from the colorant-containing solvent ingredient, thereby obtaining purified BHET; and a solvent removal step in which the solvent remaining in the crystals of the purified BHET is removed to obtain high-purity BHET.
机译:[问题]提供一种生产高纯度双(2-羟乙基)对苯二甲酸酯(BHET)的方法,通过该方法可以容易地由着色聚酯废物易于产生高纯度BHET。 [溶液]根据本发明的制备高纯度BHET的方法包括:解聚步骤,其中将彩色聚酯废料解聚以获得包括有色原油BHET的解聚产物;除去浓缩步骤,其中除去将脱聚产物中包含的低沸点成分被除去以浓缩BHET;其中来自粗BHET回收BHET的恢复步骤,得到中纯度的BHET;将中纯度BHET在脱色溶剂中进行结晶的结晶分离步骤,通过固体液体分离从含色剂的溶剂成分分离晶体,从而获得纯化的BHET;和溶剂去除步骤,其中除去待纯化的BHET晶体中的溶剂,得到高纯度的BHET。

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