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HIGH-ENTROPY RARE EARTH-TOUGHENED TANTALATE CERAMIC AND PREPARATION METHOD THEREFOR

机译:高熵稀土 - 韧性钽酸盐陶瓷和制备方法

摘要

The present invention relates to the technical field of high-entropy ceramics, and specifically disclosed is a high-entropy rare earth-toughened tantalate ceramic. The ceramic is prepared by sintering Ta205 powder and x types of different RE203 powder, wherein 4≤x≤9, and the molar ratio of the RE203 powder is 1. RE203 powder and Ta205 powder having the molar ratio of RE to Ta being 1:1 are weighed, a solvent is added for mixing, and ball milling is performed by a ball mill to obtain mixed powder M; the powder M is dried at a temperature of 650-850°C for 1.5-2 h to obtain dried powder; the powder is sieved to obtain powder N, the powder N is put in a mold for first pressing to obtain a rough blank, and the rough blank is then pressed for the second time to obtain a compact blank; the compact blank is sintered to obtain the high-entropy rare earth-toughened tantalate ceramic. The high-entropy ceramic has higher hardness and toughness.
机译:技术领域本发明涉及高熵陶瓷技术领域,具体地公开了一种高熵稀土韧性陶瓷陶瓷。 陶瓷通过烧结Ta205粉末和X种不同的RE203粉末制备,其中4≤x≤9,RE203粉末的摩尔比为1. RE203粉末和TA205粉末具有RE的摩尔比为1: 称重1,加入溶剂以混合,并通过球磨机进行球磨,得到混合粉末M; 将粉末M在650-850℃的温度下干燥1.5-2小时,得到干燥的粉末; 筛分粉末以获得粉末N,将粉末N放入模具中以首先按压以获得粗糙的坯料,然后第二次压制粗坯以获得紧凑的坯料; 紧凑的坯料被烧结以获得高熵稀土韧性的钽陶瓷。 高熵陶瓷具有更高的硬度和韧性。

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