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CONTINUOUS METHOD FOR OBTAINING A CRYSTALLINE MONOSACCHARIDE AND DEVICE FOR CONTINUOUS CRYSTALLIZATION

机译:获得结晶单糖和用于连续结晶的晶体的连续方法

摘要

The invention relates to a continuous method for obtaining a crystalline monosaccharide, comprising: continuous crystallization of the monosaccharide in a main crystallizer (10), wherein crystallization by evaporation and/or crystallization by cooling is carried out continuously on a crystal suspension in the main crystallizer in order to allow crystals of the monosaccharide to grow in the crystal suspension; separation of crystals of the monosaccharide out of the crystal suspension to obtain crystalline monosaccharide; continuous formation of a mass of crystallization magma for the main crystallizer (10) in a cascade, wherein the cascade comprises at least one first stage (13) and a final stage (15) connected in series and each stage comprises at least one pre-crystallizer (13A, 15A), wherein, in the at least one pre-crystallizer (13A) of the first stage (13), a solution is seeded with monosaccharide by means of monosaccharide seed crystals in order to obtain a pre-crystallization magma, and a mass of crystallization magma for the downstream stage (14, 15) is formed from the pre-crystallization magma by means of crystallization by cooling and/or crystallization by evaporation, and wherein a solution containing monosaccharide and a mass of crystallization magma from the upstream stage is supplied to the at least one pre-crystallizer (15A, 15B, 15C) of the final stage (15) to obtain a pre-crystallization magma, and in the at least one pre-crystallizer (15A, 15B, 15C) of the final stage (15) a mass of crystallization magma for the main crystallizer (10) is formed from the pre-crystallisation magma by means of crystallization by cooling and/or crystallization by evaporation; the continuous supply of a solution containing the monosaccharide and a mass of crystallization magma from the at least one pre-crystallizer (15A, 15B, 15C) of the final stage (15) of the cascade to the main crystallizer (10) to provide the crystal suspension.
机译:本发明涉及一种用于获得结晶单糖的连续方法,包括:在主结晶器(10)中的单糖连续结晶,其中通过冷却通过蒸发和/或结晶结晶在主结晶器中的晶体悬浮液上进行结晶为了允许单糖的晶体在晶体悬浮液中生长;将单糖的晶体分离出晶体悬浮液中以获得结晶单糖;连续形成级联中的主结晶器(10)的结晶岩浆,其中级联包括至少一个第一级(13)和串联连接的第一级(15),并且每个级包括至少一个预先结晶器(13a,15a),其中,在第一阶段(13)的至少一个预结晶器(13a)中,通过单糖种子晶体用单糖接种溶液,以获得预结晶岩浆,和下游级(14,15)的一定的结晶岩浆通过通过蒸发冷却和/或结晶来通过结晶来由预结晶岩浆形成,并且其中含有单糖的溶液和来自的一定的结晶岩浆上游阶段被供应到最终阶段(15)的至少一个预结晶器(15a,15b,15c),以获得预结晶岩浆,并且在至少一个预结晶器(15a,15b,15c)中最终阶段(15)的质量用于主结晶器(10)的Rystallization Magma通过通过蒸发冷却和/或结晶结晶来由预结晶岩浆形成;连续供应含有单糖的溶液和从级联的最终阶段(15)的至少一个预结晶器(15a,15b,15c)的结晶器(15a,15b,15c)到主结晶器(10)以提供晶体悬浮液。

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