首页> 外国专利> METHOD FOR PREPARING OXYGEN-FREE PASSIVATED TITANIUM OR TITANIUM-ALLOY POWDER PRODUCT BY MEANS OF GAS-SOLID FLUIDIZATION

METHOD FOR PREPARING OXYGEN-FREE PASSIVATED TITANIUM OR TITANIUM-ALLOY POWDER PRODUCT BY MEANS OF GAS-SOLID FLUIDIZATION

机译:通过气体固体流化制备无氧钝化钛或钛合金粉末产品的方法

摘要

A method for preparing an oxygen-free passivated titanium or titanium-alloy powder product by means of gas-solid fluidization is provided. The new method includes placing the metal halide and the titanium powder which meet formula requirements into a gasifier and a fluidized bed reactor respectively; heating the gasifier to gasify the metal halide, and introducing dry argon and halide gas into the fluidized bed reactor; opening the fluidized bed, heating the fluidized bed, fluidizing the titanium powder after the introduction of the argon and the metal halide gas, and cooling the product to obtain the titanium powder subjected to oxygen-free passivation using metal chloride; molding the oxygen-free passivated titanium powder into a green body with powder metallurgy technology; and sintering the green body in vacuum or argon atmosphere according to the molding technology, and after temperature rise treatment, performing a densification sintering operation to obtain a high-performance titanium product component.
机译:提供了一种通过气体固体流化制备无氧钝化钛或钛合金粉末产品的方法。新方法包括将金属卤化物和钛粉末分别占用成气化器和流化床反应器的金属卤化物和钛粉末。加热气化器以气化金属卤化物,并将干燥的氩气和卤化物气体引入流化床反应器中;打开流化床,加热流化床,在引入氩气和金属卤化物后流化钛粉末,并冷却产物以获得使用金属氯化物进行无含氧钝化的钛粉末;用粉末冶金技术将无氧钝化钛粉末成含有含氧的硫化物粉末;并根据成型技术,在温度升温处理后烧结生气或氩气氛,进行致密化烧结操作以获得高性能钛产物组分。

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