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MULTI-GAS MIXED LIBS SIGNAL ENHANCEMENT DEVICE AND HEAVY METAL DETECTION METHOD

机译:多气混合LIBS信号增强装置和重金属检测方法

摘要

A multi-gas mixed laser-induced breakdown spectroscopy (LIBS) signal enhancement device and a heavy metal detection method, the device comprising: a solid pulse laser (1), a light path system (2), a multi-gas mixed spherical gas chamber (3), an optical fiber collector (4), a spectrometer (5) and a controller (8). The light path system (2) is connected to the solid pulse laser (1); the multi-gas mixing spherical gas chamber (3) is arranged corresponding to the light path system (2); the optical fiber collector (4) is arranged corresponding to the multi-gas mixing spherical gas chamber (3); the spectrometer (5) is connected to the optical fiber collector (4); and the controller (8) is connected to the spectrometer (5) and the solid pulse laser (1), respectively. The spectrometer (5) determines laser-induced breakdown spectral information according to light signals received by the optical fiber collector (4); and the controller (8) determines LIBS spectrum information according to the received laser-induced breakdown spectral information. The device provides a uniform mixed environment atmosphere of various gases for plasma generated by laser ablation of a sample to be detected, and may adjust the input quantity of the gases and the proportion of air according to detection requirements, thereby enhancing the LIBS spectral information and improving the accuracy of heavy metal content determination.
机译:多气混合激光诱导的击穿光谱(Libs)信号增强装置和重金属检测方法,该装置包括:固体脉冲激光(1),光路系统(2),多气混合球形气体腔室(3),光纤收集器(4),光谱仪(5)和控制器(8)。光路系统(2)连接到固体脉冲激光器(1);多气混合球形气体室(3)对应于光路系统(2)。光纤收集器(4)对应于多气混合球形气体室(3)。光谱仪(5)连接到光纤收集器(4);并且控制器(8)分别连接到光谱仪(5)和固体脉冲激光器(1)。光谱仪(5)根据光纤收集器(4)接收的光信号来确定激光诱导的击穿光谱信息;并且控制器(8)根据接收的激光诱导的击穿光谱信息确定Libs频谱信息。该装置提供了通过激光消融待检测的样品产生的等离子体的各种气体的均匀混合环境气氛,并且可以根据检测要求调节气体的输入量和空气的比例,从而增强了Libs光谱信息和提高重金属含量测定的准确性。

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