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Method for recovering organic amine

机译:回收有机胺的方法

摘要

Liquid phase component by-produced in the method for producing a compound represented by the following general formula (I) (in the formula, R11 is an organic group having a valence of 1 to 3) and n11 is an integer of 1 or more and 3 or less) From the following, a method for recovering a compound represented by the following general formula (III) (wherein R31 is an organic group having a valence of 1 or more and a valence of 3 or less, and n31 is an integer of 1 or more and 3 or less): There is provided a recovery method including the following steps (1) to (3) or steps (A) and (B) and step (4). Step (1): A step of reacting the liquid phase component with at least one active hydrogen-containing compound in a reactor. Step (2): A step of returning the condensate obtained by cooling the gas phase component of the reactor into the reactor. Step (3): A step of discharging the gas phase components that have not been condensed in the step (2) to a place other than the reactor. Step (A): A step of mixing the liquid phase component, water and the compound represented by the general formula (III). Step (B): A step of reacting the liquid phase component and water in a reactor. Step (4): A step of discharging a reaction liquid containing the compound represented by the general formula (III) as a liquid phase component in the reactor to the outside of the reactor. [Chemical 1]
机译:通过制备由以下通式(I)表示的化合物的方法(在式中,R11是1至3的有机基团)中制备的液相组分,N11是1或更多的整数从以下3或更小中,用于回收由以下通式(III)表示的化合物的方法(其中R31是具有1或更高的合肥的有机基团,并且3或更小,N31是整数的价值提供1或更长时间和3或更低):提供了一种恢复方法,包括以下步骤(1)至(3)或步骤(a)和(b)和步骤(4)。步骤(1):将液相组分与反应器中至少一种活性氢化合物反应的步骤。步骤(2):通过将反应器的气相组分冷却到反应器中,返回所获得的冷凝物的步骤。步骤(3):排出尚未在步骤(2)中的气相组分排出的步骤(2)到反应器以外的侧面。步骤(a):将液相组分,水和由通式(III)表示的化合物混合的步骤。步骤(b):将液相组分和水反应反应物反应的步骤。步骤(4):将含有由通式(III)表示的化合物的反应液排出的步骤,作为反应器外部反应器中的液相组分。 [化学1]

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