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APPARATUS AND METHOD FOR CONTINUOUS SOLVOTHERMAL SYNTHESIS OF NANOPARTICLES

机译:用于连续溶剂热合成纳米颗粒的装置和方法

摘要

An apparatus and a method for continuous solvothermal synthesis of nanoparticles, are provided. The apparatus includes an inlet section, a reactor section, a flexible quenching unit, and an outlet section. The inlet section separately receives reactants including the solvent and a precursor solution that are allowed to flow into the reactor section. The reactor section includes multiple spiral turns such that each of the spiral turns includes a helical channel followed by a counter-helical channel for enabling mixing of the reactants to cause solvothermal reactions between them. The counter-helical channel changes the direction of flow of reactants upon flow of said reactants from the helical channel to the counter-helical channel. The flexible quenching section enclosing a portion of the reactor section quenches a slurry formed as a result of the solvothermal reactions, wherein the slurry includes the nanoparticles of targeted characteristics. The outlet section facilitates withdrawal of the slurry.
机译:提供了一种用于连续溶液合成纳米颗粒的装置和方法。该装置包括入口部分,反应器部分,柔性淬火单元和出口部分。入口部分分别接收包括溶剂和前体溶液的反应物,其允许流入反应器部分。反应器部分包括多个螺旋转动,使得每个螺旋转弯包括螺旋通道,然后包括反螺旋通道,以使反应物能够使它们之间的溶剂热反应能够使其混合。反螺旋通道在从螺旋通道到反螺旋通道的螺旋通道流动时改变反应物的流动方向。封闭反应器部分一部分的柔性淬火部分淬灭作为溶剂热反应的结果形成的浆料,其中浆料包括靶向特征的纳米颗粒。出口部分有助于撤回浆料。

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