首页> 外国专利> PURIFIED LITHIUMBIS (FLUOROSULFONYL) IMID (LIFSI) PRODUCTS, METHODS OF PURIFYING RAW LIFSI, AND USES OF PURIFIED LIFSI PRODUCTS

PURIFIED LITHIUMBIS (FLUOROSULFONYL) IMID (LIFSI) PRODUCTS, METHODS OF PURIFYING RAW LIFSI, AND USES OF PURIFIED LIFSI PRODUCTS

机译:纯化的锂锂(氟磺酰基)IMID(LIFSI)产品,纯化生利水的方法,以及纯化的LIFSI产品的用途

摘要

Method for removing target impurities from a crude lithium bis (fluorosulfonyl) imide (LiFSI) to produce a purified LiFSI product. In some embodiments, a purification method includes contacting crude LiFSI with a first anhydrous organic solvent to produce a solution containing LiFSI and the target impurity (s), wherein the LiFSI is soluble and the impurity (s) are im Is / are essentially insoluble. In some embodiments, a second anhydrous organic solvent is added to the solution to precipitate the target impurity (s), which are then filtered to obtain a filtrate. In some embodiments, solvent is removed from the filtrate to obtain a solid mass containing LiFSI, which can then be contacted with a third anhydrous organic solvent in which the LiFSI is insoluble. The LiFSI can then be isolated from the third anhydrous organic solvent to obtain the purified LiFSI product. Also disclosed are purified LiFSI products and electrochemical devices using purified LiFSI products, among others.
机译:从粗锂双(氟磺酰基)酰亚胺(Lifsi)中除去靶杂质的方法以产生纯化的LIFSI产物。在一些实施方案中,纯化方法包括使粗LiLsi与第一无水有机溶剂接触以制备含有LiFSI和靶杂质的溶液,其中Lifsi是可溶的,并且杂质是IM为/基本上不溶于。在一些实施方案中,将第二无水有机溶剂加入到溶液中以沉淀靶杂质,然后过滤以获得滤液。在一些实施方案中,从滤液中除去溶剂,得到含有LIFSI的固体物质,然后可以与第三无水有机溶剂接触,其中LIFSI不溶于不溶于溶剂。然后可以从第三无水有机溶剂中分离LIFSI,得到纯化的LIFSI产物。还公开了使用纯化的LIFSI产品的纯化的LIFSI产品和电化学装置等。

著录项

  • 公开/公告号DE112019005762T5

    专利类型

  • 公开/公告日2021-07-29

    原文格式PDF

  • 申请/专利权人 SES HOLDINGS PTE. LTD;

    申请/专利号DE20191105762T

  • 发明设计人 RAJENDRA P. SINGH;QICHAO HU;

    申请日2019-11-15

  • 分类号C01B21/086;C01B21/084;C07C303/40;H01M10/0567;

  • 国家 DE

  • 入库时间 2024-06-14 21:52:14

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