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METHOD FOR MEASURING NMR-DATA OF A TARGET SAMPLE IN AN NMR SPECTROMETER AND NMR SPECTROMETER
METHOD FOR MEASURING NMR-DATA OF A TARGET SAMPLE IN AN NMR SPECTROMETER AND NMR SPECTROMETER
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机译:测量NMR光谱仪和NMR光谱仪中靶样品NMR数据的方法
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摘要
An NMR spectrometer for carrying out the method according to any one of the preceding claims, the NMR spectrometer (1) comprising a compensation system (5) and a main field magnet (2) with main magnet poles (2a, 2b) for generating a main magnetic field (3), the compensation system (5) comprising:- at least one target sample coil (6) and a lock sample coil (7) positioned in a volume of interest (4), the volume of interest (4) being arranged between the main magnet poles (2a, 2b),- at least one compensation coil (8) for compensating a drift of the main magnetic field (3) within the volume of interest (4),- at least one target channel for generating RF-pulses with a target excitation frequency, and- a lock data treatment system (9) comprising a lock channel (12) for generating RF-pulses with a lock excitation frequency, wherein the lock data treatment system (9) is configured to adapt a compensation current in the at least one compensation coil (8) and to correct simultaneously the target frequency by applying a target frequency correction offset FCO at the target channel.;The inventive NMR spectrometer has an improved lock channel, in particular for measurements where lock coil and the target coil are to be positioned at a separate position within the volume of interest, thus being placed in different magnetic field environments.
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