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METHOD FOR MEASURING NMR-DATA OF A TARGET SAMPLE IN AN NMR SPECTROMETER AND NMR SPECTROMETER

机译:测量NMR光谱仪和NMR光谱仪中靶样品NMR数据的方法

摘要

An NMR spectrometer for carrying out the method according to any one of the preceding claims, the NMR spectrometer (1) comprising a compensation system (5) and a main field magnet (2) with main magnet poles (2a, 2b) for generating a main magnetic field (3), the compensation system (5) comprising:- at least one target sample coil (6) and a lock sample coil (7) positioned in a volume of interest (4), the volume of interest (4) being arranged between the main magnet poles (2a, 2b),- at least one compensation coil (8) for compensating a drift of the main magnetic field (3) within the volume of interest (4),- at least one target channel for generating RF-pulses with a target excitation frequency, and- a lock data treatment system (9) comprising a lock channel (12) for generating RF-pulses with a lock excitation frequency, wherein the lock data treatment system (9) is configured to adapt a compensation current in the at least one compensation coil (8) and to correct simultaneously the target frequency by applying a target frequency correction offset FCO at the target channel.;The inventive NMR spectrometer has an improved lock channel, in particular for measurements where lock coil and the target coil are to be positioned at a separate position within the volume of interest, thus being placed in different magnetic field environments.
机译:一种NMR光谱仪,用于执行根据前述权利要求中任一项的方法,包括补偿系统(5)和主磁场磁体(2)的NMR光谱仪(1),其具有用于产生A的主磁极(2a,2b)主磁场(3),补偿系统(5)包括: - 至少一个目标样品线圈(6)和位于感兴趣的体积(4)的锁定样本线圈(7),感兴趣的体积(4)布置在主磁极(2a,2b)之间, - 至少一个补偿线圈(8),用于在感兴趣的体积内补偿主磁场(3)的漂移(4), - 至少一个目标通道,用于产生具有目标激发频率的RF脉冲,以及 - 锁定数据处理系统(9),包括用于产生具有锁激励频率的RF脉冲的锁定通道(12),其中锁定数据处理系统(9)被配置为使所述至少一个补偿线圈中的补偿电流适应补偿电流(8)并通过在目标通道上应用目标频率校正偏移FCO同时校正目标频率。;本发明的NMR光谱仪具有改进的锁管,特别是用于锁定线圈和目标线圈的测量值。在感兴趣的体积内的单独位置,从而放置在不同的磁场环境中。

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