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INTELLIGENT CHEMICAL REACTION DEVICE AND SAMPLING METHOD

机译:智能化学反应装置和取样方法

摘要

An intelligent chemical reaction device and a sampling method, comprising: a sampling temporary storage chamber (3) and a reaction stirring chamber (4). A peristaltic pump (32) is mounted at the top of the sampling temporary storage chamber (3); a placing rack (34) is placed in a cavity under the peristaltic pump (32); a liquid level sensor (33) is mounted on the placing rack (34); a light source (43) is mounted at the top of the reaction stirring chamber (4); an automatic stirrer (5) is placed in a cavity under the light source (43); the peristaltic pump (32) is connected to a sampling test tube (35) and a reaction container (53) by means of hoses, separately. The method comprises the steps: S1. sampling parameter obtaining: according to a fit curve, determining that a reaction type R in sampling parameters is a zero-level or first-level reaction; S. sampling of the zero-level reaction; S3. sampling of the first-level reaction; S4. sampling time adjustment. According to the device, the peristaltic pump (32) is configured to take a sample, and the sampling precision is high; the automatic stirrer (5), a timer, and the liquid level sensor (33) are used for automatic sampling and storage, and labor and material resources are saved. By means of the method, sampling time is controllable and reasonable.
机译:智能化学反应装置和采样方法,包括:采样临时储存室(3)和反应搅拌室(4)。蠕动泵(32)安装在采样临时储存室(3)的顶部。将放置齿条(34)放置在蠕动泵(32)下的腔内;液位传感器(33)安装在放置架上(34)上;光源(43)安装在反应搅拌室(4)的顶部。将自动搅拌器(5)放置在光源(43)下的腔内;蠕动泵(32)通过软管分别连接到采样试管(35)和反应容器(53)。该方法包括步骤:S1。采样参数获取:根据拟合曲线,确定采样参数中的反应类型R是零级或第一级反应; S.零水平反应的抽样; S3。第一级反应的抽样; S4。采样时间调整。根据该装置,蠕动泵(32)配置成采用样品,采样精度高;自动搅拌器(5),计时器和液位传感器(33)用于自动采样和存储,并且节省了劳动力和材料资源。通过该方法,采样时间可控且合理。

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