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Particles for bonding material and manufacturing method thereof, bonding paste and preparation method thereof, and manufacturing method of bonded body

机译:用于粘合材料的颗粒及其制造方法,粘合浆料及其制备方法,以及粘合体的制造方法

摘要

As for the particles for bonding material, an organic protective film is formed on the surface of the copper nanoparticles, the BET specific surface area is 3.5 m 2 /g or more and 8 m 2 /g or less, and the BET diameter is in each range of 80 nm or more and 200 nm or less, and the organic protective film is bonded It is contained in the range of 0.5 mass % or more and 2.0 mass % or less with respect to the particle|grains for materials. When particles for a bonding material were analyzed using time-of-flight secondary ion mass spectrometry (TOF-SIMS), the detected amounts of C 3 H 3 O 3− ions and C 3 H 4 O 2−ions were Cu + It is in the range of 0.05 times or more and 0.2 times or less with respect to the detection amount of ions, and the detection amount of C 5 or more ions is in the range of less than 0.005 times the detection amount of Cu + ions.
机译:对于用于粘合材料的颗粒,在铜纳米颗粒的表面上形成有机保护膜,BET比表面积为3.5m 2 / g以上且8m 2 / g或更低,并且BET直径在80nm以上且200nm或更小的每个范围,并且有机保护膜键合在0.5质量%或更多和2.0质量%或更小的范围内,相对于材料的颗粒含量。使用飞行时间二次离子质谱(TOF-SIMS)进行分析用于粘合材料的颗粒,检测量的 c 3 h 3 O 3 - 离子和c 3 h 4 O 2 - 离子是Cu + 相对于检测量的离子和检测量为0.05或更大的0.05倍或更大,以及C 5 的检测量。更多离子在检测量的Cu +离子的范围内的范围内。

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