Process for making mono or di-ammonium phosphate according to the parent patent gives better yields when an ammonium salt is added to the mixture of solvent and crude phosphoric acid solution at the extraction stage. In an example various amounts of crude phosphoric acid were partitioned between water and isobutanol, in the presence or absence of 15% NH4NO3, and the partition coefficients calculated. In all cases more P2O5 went into the solvent when NH4NO3 was present.
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机译:当在萃取阶段将铵盐添加到溶剂和粗磷酸溶液的混合物中时,根据母专利的制备磷酸一铵或二铵的方法可获得更好的产率。在一个实例中,在存在或不存在15%NH 4 NO 3的情况下,将各种量的粗磷酸在水和异丁醇之间分配,并计算分配系数。在所有情况下,当存在NH4NO3时,会有更多的P2O5进入溶剂。
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