首页> 外国专利> PROCESS FOR SELECTIVELY PURIFYING SUGAR BEET DIFFUSION JUICE AND BY-PRODUCT RECOVERY OF VALUABLE ORGANIC ACIDS THEREFROM

PROCESS FOR SELECTIVELY PURIFYING SUGAR BEET DIFFUSION JUICE AND BY-PRODUCT RECOVERY OF VALUABLE ORGANIC ACIDS THEREFROM

机译:选择性提纯甜菜扩散汁的工艺以及由此而来的有价值的有机酸的副产品回收

摘要

A process for selectively purifying sugar beet diffusion juice in which the raw diffusion juice is first neutralized to minimize inverted sugar formation and stabilize the colloidal content without precipitating the soluble organic acids. The neutralized diffusion juice is then subjected to high centrifugal forces to separate the colloidal and particulate content from the diffusion juice. After the colloidal and particulate solids are removed, the clarified diffusion juice is contacted with a stoichiometric equivalent or slight excess of lime based upon the soluble organic acid concentration in the diffusion juice to react with the soluble organic acids to form insoluble calcium salts of the organic acids. The insoluble calcium salts of the organic acids are then removed from the diffusion juice. The diffusion juice may be further purified as needed. The insoluble calcium salts of the organic acids are then placed in an aqueous solution such as hot water. Carbon dioxide gas or other suitable carbonate ion producing agent is dissolved in the hot water to release the organic acids and produce a calcium carbonate precipitate. The dissolved organic acids are then selectively recovered by conventional means.
机译:一种选择性纯化甜菜扩散汁的方法,其中首先中和粗制扩散汁,以最大程度地减少倒糖的形成并稳定胶体含量,而不会沉淀可溶性有机酸。然后使中和的扩散汁经受高离心力以从扩散汁中分离胶体和颗粒含量。除去胶体和颗粒状固体后,使澄清的扩散汁与化学计量当量或略微过量的石灰接触(基于扩散汁中的可溶性有机酸浓度),以与可溶性有机酸反应形成有机物的不溶性钙盐酸。然后从扩散汁中除去有机酸的不溶性钙盐。扩散汁可以根据需要进一步纯化。然后将有机酸的不溶性钙盐放入水溶液如热水中。将二氧化碳气体或其他合适的碳酸根离子产生剂溶解在热水中以释放有机酸并产生碳酸钙沉淀。然后通过常规方法选择性地回收溶解的有机酸。

著录项

  • 公开/公告号US3734773A

    专利类型

  • 公开/公告日1973-05-22

    原文格式PDF

  • 申请/专利权人 HALEY BUS;

    申请/专利号USD3734773

  • 发明设计人 HALEY BUS;

    申请日1971-08-02

  • 分类号C07C53/00;C07C55/00;C13D3/00;

  • 国家 US

  • 入库时间 2022-08-23 06:28:36

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