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process and plant for de purare and condense gas reaction in the production of hydrofluoric acid

机译:氢氟酸生产中的纯水和冷凝气反应的方法和装置

摘要

The present invention relates to a process for recovering hydrogen fluoride from the gaseous reaction product of a metal fluoride with sulfuric acid by washing the gaseous product in a first stage with concentrated sulfuric acid and thereby cooling the gas to a temperature of about 60 DEG to 130 DEG C, cooling said gas by indirect heat exchange with water to a temperature of about 30 DEG to 50 DEG C in a second stage and in a third stage by direct heat exchange with pure hydrofluoric acid to a temperature of about 20 DEG to 25 DEG C, condensing hydrogen fluoride in the cooled gaseous product of the third stage in at least two additional stages and recovering condensed hydrogen fluoride.
机译:本发明涉及一种从金属氟化物与硫酸的气态反应产物中回收氟化氢的方法,该方法是在第一阶段用浓硫酸洗涤气态产物,然后将其冷却至约60-130℃。在第二阶段中通过与水间接热交换至约30-50℃的温度来冷却所述气体,在第三阶段中通过与纯氢氟酸直接热交换至约20-25℃的温度来冷却所述气体。 C,在至少另外两个步骤中使第三阶段的冷却的气态产物中的氟化氢冷凝,并回收冷凝的氟化氢。

著录项

  • 公开/公告号IT977557B

    专利类型

  • 公开/公告日1974-09-20

    原文格式PDF

  • 申请/专利权人 BAYER AG;

    申请/专利号IT19730048509

  • 发明设计人

    申请日1973-02-28

  • 分类号C01B;

  • 国家 IT

  • 入库时间 2022-08-23 06:04:08

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