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A method for the production of 7 - chlorine - 1,3 - dihydropyridines - 1 - methyl - 5 - phenyl - 2h - 1,4 - benzodiazepine - 2 - on
A method for the production of 7 - chlorine - 1,3 - dihydropyridines - 1 - methyl - 5 - phenyl - 2h - 1,4 - benzodiazepine - 2 - on
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机译:一种生产7-氯-1,3-二氢吡啶-1-甲基-5-苯基-2h-1,4-苯并二氮杂-2-的方法。
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摘要
of formula (I) (where R1=H, Me, Et, Pr or cyclopropyl, and R2 =H, halo, NO2, or CH2F, are prepd by an improved method consisting of self-condensation of a 2-(2-haloacetamido)-5-substd benzophenone. in the presence of (CH2)6N4. The reactions is carried out in EtOH opt. contng. HCl and up to 15% H2O, above 50 degrees. The intermediate (CH2)6N4 salt may be isolated. (I) are sedatives and hypnotics.
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