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Thermally controlled microscope stage assembly

机译:热控显微镜镜台组件

摘要

A thermally controlled microscope stage assembly for use in measuring transformation temperatures between -180° and +600°C. The stage assembly includes a thick-walled platen with a resistance heater in an annular cavity adjacent a specimen chamber and a cooling channel arranged along the periphery of the platen for, respectively, heating and cooling the specimen chamber. The platen has a lighting well disposed along the optical axis of the associated microscope. A condenser is built in the lighting bore and includes a pair of axially spaced plano- spherical fused quartz lenses both with their spherical surface facing the incident illuminating beam. The lens closer to the microscope has its plane surface, which defines its isophote plane, level with the upper surface of the platen. The specimen chamber is defined by the top surface of the platen, a thick-walled annular member seated on the platen and a thin transparent plate member. The temperature in the specimen chamber is measured by a platinum resistance probe which forms one arm of a linearizer bridge. A heating relay and a cooling relay are connected respectively in series with heating and cooling supplies and a thermostat control selectively controlling one of the relays in response to the sign of the voltage difference between the output voltage of the linearizer bridge and a set voltage determined by an adjustable voltage source corresponding to the set temperature.
机译:一种热控显微镜镜台组件,用于测量-180°至+ 600°C之间的转变温度。载物台组件包括厚壁的压板,该压板在与样品室相邻的环形腔中具有电阻加热器,以及沿着压板的外围布置的冷却通道,其分别用于加热和冷却样品室。压板具有沿相关显微镜的光轴布置的照明井。聚光器内置在照明孔中,并包括一对轴向隔开的平球熔融石英透镜,它们的球面均面向入射照明光束。离显微镜更近的透镜的平面定义了等渗平面,该平面与压板的上表面齐平。样品室由压盘的顶表面,位于压盘上的厚壁环形构件和薄的透明板构件限定。样品室中的温度由铂电阻探针测量,该探针形成线性化桥的一个臂。加热继电器和冷却继电器分别与加热和冷却电源串联连接,并且恒温器控制根据线性化电桥的输出电压与由以下公式确定的设定电压之间的电压差的符号,选择性地控制其中一个继电器与设定温度相对应的可调电压源。

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