首页>
外国专利>
Distillation process for recovery of hexamethyl disiloxane
Distillation process for recovery of hexamethyl disiloxane
展开▼
机译:回收六甲基二硅氧烷的蒸馏方法
展开▼
页面导航
摘要
著录项
相似文献
摘要
There is disclosed an azeotropic distillation process for separating and recovering hexamethyl disiloxane (HMDO) from toluene in a spent liquor mixture. An HMDO azeotrope former, pyrrolidone, is added to the liquor. The pyrrolidine is added in an amount of at least about 1.81 parts by weight per 1.0 part by weight of HMDO. Preferably, it is added in excess, as about 2.7 to about 5.4 parts by weight of pyrrolidine per 1. 0 part by weight of HMDO. The resulting azeotrope of HMDO and pyrrolidine is then separated by distillation from the liquor. The pyrrolidine may be subsequently recovered from the HMDO by extraction with water. Other HMDO azeotrope formers, such as tertiary butanol, may also be utilized.
展开▼