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METHOD FOR PREPARING DELTA2 OR DELTA3-CEPHALOSPORINE SULPHOXIDES BY OXIDATION OF DELTA2 OR DELTA3-CEPHALOSPORINE COMPOUNDS
METHOD FOR PREPARING DELTA2 OR DELTA3-CEPHALOSPORINE SULPHOXIDES BY OXIDATION OF DELTA2 OR DELTA3-CEPHALOSPORINE COMPOUNDS
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机译:通过氧化DELTA2或DELA3-西酞菁化合物制备DELTA2或DELA3-西酞菁碱的方法
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1,260,697. Cephalosporin sulphoxides. ELI LILLY & CO. 24 July, 1969 [3 Oct., 1968], No. 37342/69. Heading C2A. A process for the oxidation of a cephalosporin to a cephalosporin sulphoxide comprises treating the cephalosporin with at least one equivalent of an oxidizing agent at a temperature in the range of - 50‹ to + 100‹ C., the oxidizing agent being selected from inorganic peracids having a reduction potential of at least + 1À5 volts and containing only non-metallic elements, organic carboxylic peracids, and mixtures of hydrogen peroxide and an acid having a dissociation constant of at least 10SP-5/SP.
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机译:1,260,697。头孢菌素亚砜。 ELI LILLY&CO。1969年7月24日[1968年10月3日],编号37342/69。标题C2A。将头孢菌素氧化为头孢菌素亚砜的方法包括在-50℃至+ 100℃的温度下,用至少一当量的氧化剂处理头孢菌素,所述氧化剂选自无机过酸。还原电势至少为+ 1〜5伏,并且仅包含非金属元素,有机羧酸过酸以及过氧化氢和解离常数至少为10 -5 SP>的酸的混合物。
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