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HIGHLY SENSITIVE FLAME PHOTOMETER TYPE ANALYZER

机译:高灵敏度火焰光度计型分析仪

摘要

PURPOSE:To detect arsine, phosphine and diborane in high sensitivity, by introducing sample gas to the fuel additive air side and sending into the burner part and then, exciting in an atmosphere of oxidizing flame always. CONSTITUTION:Sample gas (e.g. arsine, phosphine and diborane etc. in a room atmosphere) is jetted from the lower part of a burner part 2 by a sample gas introducing apparatus 1. On one hand, a fuel gas hydrogen 3 is mixed with a nitrogen 4 and hereafter, gaseous mixture is jetted from the tip end of a jet nozzle 5 and a hydrogen flame is formed by ignition. When said poisonous gas such as the arsine, phosphine and diborane exists in the sample gas, a peculiar neutral molecular emission spectrum is emitted. Then, this sepectrum is caught by a multiplier phototube 7 connected to a high voltage power source 8 and is amplified. Moreover, it is amplified by a preamplifier 9 and a main amplifer 10 and hereafter, an indicating response is recorded on a recorder 11.
机译:目的:以高灵敏度检测gas,膦和乙硼烷,方法是将样气引入燃料添加剂空气侧,送入燃烧器部件,然后始终在氧化火焰气氛中激发。组成:通过样气导入装置1从燃烧器部件2的下部喷射样气(例如,室内大气中的砷化氢,膦和乙硼烷等)。一方面,将燃料气中的氢气3与氮气4和此后,从喷嘴5的尖端喷射出气体混合物,并且通过点火形成氢火焰。当样气中存在有毒气体(如rs,磷化氢和乙硼烷)时,会发射出特殊的中性分子发射光谱。然后,该频谱被连接到高压电源8的倍增光电管7捕获并被放大。此外,它由前置放大器9和主放大器10放大,此后,指示响应被记录在记录器11上。

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