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PROCESS FOR THE MANUFACTURE OF FINELY DISPERSED SPARINGLY SOLUBLE SALTS OF OXYACIDS OF PHOSPHORUS

机译:磷的精细分散的微溶盐的制备方法

摘要

ABSTRACT OF THE DISCLOSUREThe invention relates to a process for making a finely dispersed,sparingly soluble salt of an oxyacid of phosphorus, having a maximum parti-cle size of 20 µm, by reacting a compound of a divalent metal with the oxy-acid of phosphorus or an alkali metal or ammonium salt thereof. More partic-ularly, finely dispersed salt consisting to an extent of at least 90% of par-ticles with a size between 0.05 and 7 µm is made. To this end, an at least5% by weight aqueous solution or suspension of a compound of a divalent metalselected from the group Mg, Ca, Sr, Ba, Mn, Zn, Cu, Cd, Pb, Sn, Co and Ni isreacted, while maintaining a pH range of between 3 and 9 and while stirring,with an at least 2 mol% solution of at least one trivalent metal selectedfrom the group Al, Fe and Cr in the oxyacid of phosphorus and, optionally,with an aqueous solution of an alkali metal or ammonium salt of the oxyacidof phosphorus, and the precipitated salt is separated off and dried.
机译:披露摘要本发明涉及一种制备精细分散的方法,磷含氧酸的微溶盐,具有最大的通过使二价金属的化合物与磷的酸或其碱金属或铵盐。更具体-通常,细分散的盐的含量至少为标准盐的90%制成的刻度线的尺寸在0.05到7 µm之间。为此,至少5重量%的二价金属化合物的水溶液或悬浮液选自Mg,Ca,Sr,Ba,Mn,Zn,Cu,Cd,Pb,Sn,Co和Ni反应,同时保持3至9的pH范围,并在搅拌的同时,至少2 mol%的至少一种三价金属溶液在磷的含氧酸中选自Al,Fe和Cr,并且用碱金属或含氧酸铵盐的水溶液分离磷并沉淀出的盐并干燥。

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