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METHOD FOR PRODUCING PERYLENE-3,4,9,10-TETRACARBONIC ACID-N, N'-DIALKYL-DIIMID PIGMENTS

机译:丙烯-3,4,9,10-四碳烯酸-N,N'-二烷基二酰亚胺颜料的制备方法

摘要

The invention relates to a process for the preparation of perylene-3,4,9,10-tetracarboxylic acid N,N'-dialkyldiimides by reacting perylene-3,4,9,10-tetracarboxylic acid dianhydride with an alkylamine in aqueous suspension at a low temperature, in the course of which the bis-(alkylammonium) salt of perylene-3,4,9,10-tetracarboxylic acid bis-N-alkylamide is formed. The latter is reacted with a metal salt to give the corresponding sparingly soluble metal salt, which is subjected to the cyclization reaction at an elevated temperature. The pigments prepared by the process according to the invention are distinguished by high purity and are suitable for pigmenting lacquers and plastic compositions.
机译:本发明涉及一种在水悬浮液中使per-3,4,9,10-四羧酸二酐与烷基胺反应,制备the-3,4,9,10-四羧酸N,N'-二烷基二酰亚胺的方法在低温过程中,形成per-3,4,9,10-四羧酸双-N-烷基酰胺的双-(烷基铵)盐。后者与金属盐反应,得到相应的微溶金属盐,将其在升高的温度下进行环化反应。通过根据本发明的方法制备的颜料的特征在于高纯度,并且适用于给漆和塑料组合物着色。

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