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PROCESS FOR THE ISOLATION FROM NEEM OIL OF ACTIVE PRINCIPLES EVINCING OVIPOSITION DETERRENT ACTIVITY IN INSECTS

机译:从NEEM油中分离有效成分以促进昆虫驱卵活性的方法

摘要

Process for the isolation from neem oil of active principles evincing oviposition deterrent activity in insects which comprises extracting neem seed oil with an organic solvent of the kind described herein, concentrating the extract,  subjecting the concentrated extract to column chromatography over silica gel in order to fractionate it into a number of portions, re-chromatographing the first of said portions into at least twenty fractions, collecting the middle fractions, separating by filtration the solid content of said collected fractions, acetylating said filtered solid, removing the acetylated product in any known manner and recovering the non-acetylated residue as the desired active principle.
机译:从ne树油中分离出具有昆虫威慑作用的活性成分的方法,该方法包括用本文所述类型的有机溶剂提取ne树籽油,浓缩提取物,将浓缩的提取物在硅胶上进行柱色谱以分级分离。将其分为多个部分,将所述部分中的第一部分重新色谱分离成至少二十个馏分,收集中间馏分,通过过滤分离所述收集的馏分的固体成分,对所述过滤的固体进行乙酰化,以任何已知方式去除乙酰化产物并回收非乙酰化残基作为所需的活性成分。

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