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METHOD FOR THE PRODUCTION OF M-NITROBENZOESAEUREMETHYLESTER

机译:间硝基苯磺酸钠的生产方法

摘要

Methyl m-nitrobenzoate is prepared by a process in which an isomer mixture is treated with from 10 to 1000% by weight of water in the presence of from 0.05 to 20% by weight of an emulsifier, the percentages being based on the weight of the isomer mixture, (a) in a first stage at from 55 DEG to 100 DEG C. and a pH from 2 to 8 and then (b) in a second stage at from 10 DEG to 40 DEG C. and a pH of not less than 9. The methyl m-nitrobenzoate obtainable by the process of the invention is a useful starting material for the preparation of dyes and crop protection agents.
机译:间硝基苯甲酸甲酯是通过以下方法制备的:将异构体混合物在0.05至20重量%的乳化剂存在下,用10至1000重量%的水处理。异构体混合物,(a)第一步在55℃至100℃,pH为2至8,然后(b)第二步在10℃至40℃,pH不小于可通过本发明的方法得到的间硝基苯甲酸甲酯的含量高于9。9是用于制备染料和农作物保护剂的有用的起始原料。

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