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Process for preparing concentrated aqueous solutions of quaternized products from tertiary amino alkyl esters or amides of acrylic or methacrylic acids

机译:由丙烯酸或甲基丙烯酸的叔氨基烷基酯或酰胺制备季铵化产物浓缩水溶液的方法

摘要

Concentrated aqueous solutions of quaternization products of tertiary aminoalkyl esters or tertiary aminoalkylamides of acrylic or methacrylic acid are prepared by reaction of the corresponding esters or amides with an alkylating agent in a water-soluble ketone as solvent, by a process wherein, in order to isolate the quaternization product, an amount of water is added to the reaction mixture such that two phases form, and the lower aqueous phase, which contains the quaternization product in solution, is separated from the upper phase, which contains the ketone and residual alkylating agent.
机译:丙烯酸或甲基丙烯酸的叔氨基烷基酯或叔氨基烷基酰胺的季铵化产物的浓水溶液是通过使相应的酯或酰胺与烷基化剂在水溶性酮作为溶剂中反应而制备的,该方法为了分离在季铵化产物中,向反应混合物中加入一定量的水,以形成两相,并且将下部溶液中含有季铵化产物的水相与上部相分离,后者将含有酮和残留的烷基化剂。

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