首页> 外国专利> Methods for preparing cubic boron nitride sintered body and cubic boron nitride, and method for preparing boron nitride for use in the same

Methods for preparing cubic boron nitride sintered body and cubic boron nitride, and method for preparing boron nitride for use in the same

机译:立方氮化硼烧结体和立方氮化硼的制备方法,以及用于该方法的氮化硼的制备方法

摘要

There are disclosed methods for preparing cubic boron nitride sintered body. One method involves pyrolyzing borazine and/or a borazine derivative to obtain a boron nitride; mixing said boron nitride and a catalyst composed of a metal and/or metallic compound; and reacting the mixture at a pressure of 3 GPa or more and at a temperature of 700° C. or more. Another method comprises the step of pyrolyzing borazine and/or a borazine derivative to obtain a boron nitride; mixing said boron nitride and a catalyst composed of a metal and/or metallic compound; reacting the mixture at a pressure of 3 GPa or more and at a temperature of 700° C. or more; and removing the catalyst from a formed product. The conversion rate into cubic boron nitride achieved with these methods is as high as 100%, and the obtained cubic boron nitride is highly pure and fine. Also disclosed is a method for preparing boron nitride by pyrolyzing at least one compound selected from the group consisting of borazine and/or a borazine derivative at a temperature of 150° to 700° C. and a pressure of 10 MPa or more.
机译:公开了制备立方氮化硼烧结体的方法。一种方法涉及热解硼嗪和/或硼嗪衍生物以获得氮化硼。将所述氮化硼与由金属和/或金属化合物组成的催化剂混合;使混合物在3GPa以上的压力和700℃以上的温度下反应。另一种方法包括热解硼嗪和/或硼嗪衍生物以获得氮化硼的步骤;和将所述氮化硼与由金属和/或金属化合物组成的催化剂混合;使混合物在3GPa或更高的压力和700℃或更高的温度下反应;从成型产物中除去催化剂。通过这些方法获得的立方氮化硼的转化率高达100%,并且所获得的立方氮化硼是高纯度且精细的。还公开了通过在150℃至700℃的温度和10MPa或更高的压力下热解选自硼嗪和/或硼嗪衍生物中的至少一种化合物来制备氮化硼的方法。

著录项

  • 公开/公告号US4545968A

    专利类型

  • 公开/公告日1985-10-08

    原文格式PDF

  • 申请/专利权人 TOSHIBA TUNGALOY CO. LTD.;

    申请/专利号US19840667802

  • 发明设计人 SHIN-ICHI HIRANO;SHIGEHARU NAKA;

    申请日1984-11-02

  • 分类号C01B21/06;

  • 国家 US

  • 入库时间 2022-08-22 07:51:52

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