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Process for the preparation of halogen-substituted benzoylacetonitriles, 1-chloro-2(2,4-dichloro-5-fluorophenyl)ethane-2-one and its preparation
Process for the preparation of halogen-substituted benzoylacetonitriles, 1-chloro-2(2,4-dichloro-5-fluorophenyl)ethane-2-one and its preparation
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机译:卤素取代的苯甲酰基乙腈,1-氯-2(2,4-二氯-5-氟苯基)乙烷-2-酮的制备方法及其制备
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摘要
The present invention relates to a novel process for the preparation of halogen-substituted benzoylacetonitriles of the formula IMAGE in which X1 and X2 are identical or different and represent hydrogen or halogen and X3 represents halogen, which is characterised in that 1-chloroacetophenone of the formula (II) IMAGE in which X1, X2 and X3 have the abovementioned meanings, are reacted with water-soluble alkali metal cyanides in the presence of diluents and the mixture is subsequently acidified with a mineral acid, and to 1-chloro-2-(2,4-dichloro-5-fluorophenyl)ethan-2-one, which is novel, and to a process for its preparation.
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