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Method of producing sinterable powders of silicon carbide and/or boron carbide

机译:生产碳化硅和/或碳化硼可烧结粉末的方法

摘要

The invention is a process for the manufacture of sinterable silicon carbide and/or boron carbide powders having a maximum particle size of 1 mu m and finer. The process is carried out by wet grinding in aqueous suspension using mills charged with a grinding medium and with the addition of antioxidants in the presence of surfactants and subsequent wet chemical treatment with an aqueous potassium hydroxide solution. The wet grinding can be carried out, for example, with the addition of hydroquinone in the presence of quaternary ammonium salts and the wet chemical treatment with a 5-50% by weight aqueous potassium hydroxide solution under normal pressure at temperatures in the range of from room temperature to the boiling temperature of the reaction mixture or under elevated pressure at temperatures of up to 300 DEG C.
机译:本发明是用于制造最大粒径为1μm或更细的可烧结的碳化硅和/或碳化硼粉末的方法。该方法通过使用装有研磨介质并在表面活性剂存在下加入抗氧化剂的磨机在含水悬浮液中进行湿磨,然后用氢氧化钾水溶液进行湿化学处理来进行。湿法研磨可以例如在季铵盐的存在下加入对苯二酚并在常压下于约200℃至约200℃的温度下用5-50重量%的氢氧化钾水溶液进行湿法化学处理。室温至反应混合物的沸腾温度或在高达300℃的高温下。

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