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METHOD OF MEASURING SOFTENING MELTABILITY OF COAL ADDED WITH PITCH OR THE LIKE

机译:沥青或类似煤添加的煤的软化熔融性的测量方法

摘要

PURPOSE:To judge softening meltability of samples by a method wherein a sample added and blended with pitch or the like and loaded in a sample cell is heated with a constant heating rate while being pressed, thereby to measure contraction displacement. CONSTITUTION:A sample is prepared such that pitch or the like of a given amount is added to coal and then mixed to be uniformalized. Next, 40mg of this sample is loaded in a sample cell 5, which is set in an electric furnace 1 at a given position where the lower surface of a measuring rod 3 comes into contact with the upper surface of a sample 4. While supplying nitrogen gas 11 into the electric furnace 1, electric power is fed to a heating element to heat the temperature within the electric furnace 1 up to 600 deg.C at a heating rate 10 deg.C/min. During this heating process, data on changes in temperature as well as contraction displacement of the sample 4 due to the resultant softening fusion of the sample 4 are output to a recording unit 9.
机译:用途:通过以下方法判断样品的软化熔融性:将以沥青等添加并混合并装入样品室中的样品在受压的同时以恒定的加热速率加热,从而测量收缩位移。组成:准备一个样品,将一定量的沥青等添加到煤中,然后混合均匀。接下来,将40mg的该样品装载到样品室5中,该样品室5被设置在电炉1中的给定位置,在该位置处测量杆3的下表面与样品4的上表面接触。气体11进入电炉1,电力被馈送到加热元件以以10℃/ min的加热速率将电炉1内的温度加热到600℃。在该加热过程中,关于温度变化以及由于样品4的软化融合而导致的样品4的收缩位移的数据被输出到记录单元9。

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