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Process for the preparation of gamma-undecalactone from omega-undecylenoic acid

机译:由ω-十一碳烯酸制备γ-十一内酯的方法

摘要

Known processes involve large amounts of concentrated sulphuric acid as catalyst, where a variety of undesirable side-reactions take place while imparting a dark colour to the product, and several washing steps being required. The novel process is intended to result in a pure product while reducing the washing steps. The present process employs strongly acidic ion exchangers which are stable under reaction conditions. The process is less complicated and provides good yields. Preparation of gamma-undecalactone for the manufacture of odoriferous substances.
机译:已知的方法涉及大量的浓硫酸作为催化剂,其中发生多种不希望的副反应,同时给产物赋予深色,并且需要几个洗涤步骤。该新颖方法旨在在减少洗涤步骤的同时产生纯净的产品。本方法使用在反应条件下稳定的强酸性离子交换剂。该方法不那么复杂并且提供了良好的产率。制备γ-十一内酯,用于制造有味物质。

著录项

  • 公开/公告号EP0293659A2

    专利类型

  • 公开/公告日1988-12-07

    原文格式PDF

  • 申请/专利权人 HULS AKTIENGESELLSCHAFT;

    申请/专利号EP19880107780

  • 发明设计人 GUDE FRITZ DR.;WINTER ROLF;

    申请日1988-05-14

  • 分类号C07D307/32;

  • 国家 EP

  • 入库时间 2022-08-22 06:35:18

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