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Process for the isolation of high-purity tri-calcium citrate from aqueous solutions containing citric acid
Process for the isolation of high-purity tri-calcium citrate from aqueous solutions containing citric acid
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机译:从柠檬酸水溶液中分离高纯度柠檬酸三钙的方法
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摘要
1. Method of isolating highly pure crystalline tricalciumcitrate-tetrahydrate by addition of a calcium-containing precipitant to citric-acid-containing aqueous solutions at elevated temperature, which method is characterised in that, after addition of about 25 to 30% of the stoichiometrically calculated amount of calcium-containing precipitant, to the aqueous solution, required for the formation of tricalcium-citrate, the further addition is continued at a reduced rate until the first appearance of cloudiness due to tricalcium-citrate-tetrahydrate precipitating by crystallisation, then is interrupted as long as crystallisation is substantially completed and the remaining portion of the calcium-containing precipitant is added upon expiration of that period of time.
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