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Chitansanjirukonsannamaribifunmatsunoseiho

机译:C Hi谈三级入口ONS Anna马日比扶南码头是uno SEI ho

摘要

PURPOSE:To easily produce the titled readily sintering fine powder having prescribed composition, by precipitating 3-kinds of elements (Pr, Zr and Ti) in =2 steps from aqueous solutions containing each element under radiation of ultrasonic wave. CONSTITUTION:An aqueous solution containing compounds of one or more elements selected from Pb, Zr and Ti [e.g. ZrO(NO3)2 and TiCl4] is dripped into excess precipitation liquid (e.g. ammonia water) in an ultrasonic bath under stirring to form a precipitate [e.g. hydroxides of Zr and Ti] containing the above 1-2 kinds of elements. An aqueous solution containing compounds of remaining 2-1 kinds of elements of the above 3-kinds of elements (e.g. lead nitrate) is dripped into the liquid containing the precipitation liquid containing the (co)precipitate in dispersed state in the ultrasonic bath. If necessary, the precipitation operation is repeated several times until the 3-kinds of elements are completely precipitated. The precipitate containing the 3-kinds of elements is calcined at 550-750 deg.C to obtain the titled fine powder having a composition of formula I (0.9=x=1.2; 0.1=A=0.98).
机译:目的:通过在超声波辐射下从含有每种元素的水溶液中以≥= 2步的方式沉淀出3种元素(Pr,Zr和Ti),以容易地生产具有规定组成的标题易烧结细粉。组成:含有一种或多种选自Pb,Zr和Ti的元素的化合物的水溶液[例如在搅拌下将ZrO(NO3)2和TiCl4]滴加到超声浴中的过量沉淀液(例如氨水中)中以形成沉淀[例如NaCl]。 Zr和Ti]的氢氧化物含有上述1-2种元素。在超声波浴中,将包含上述3种元素中剩余的2-1种元素的化合物(例如硝酸铅)的水溶液滴加到包含具有(共)沉淀物的沉淀液的分散液中。如果需要,将沉淀操作重复几次,直到3种元素完全沉淀。将含有3种元素的沉淀物在550-750℃下煅烧,以获得具有式I的组成(0.9≤x≤1.2;0.1≤A≤0.98)的标题细粉。

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