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OXIDATION PROCESS IN THE PREPARATION OF HYDROGEN PEROXIDE BY THE ANTHRAQUINONE METHOD

机译:蒽醌法制备过氧化氢的氧化过程

摘要

In order to carry out an oxidation enclosed circuit for the production of hydrogen peroxyde by using the anthraquinone process, according to which an oxidant gas is passed on a hydrogenated solution in a parallel-flow reactor at a temperature below 100oC, at a pressure lower than 15 bar and by increasing the reaction speed in the oxidation step, the hydrogenated solution is intensively mixed after the hydrogenation step with an oxidant gas under formation of a system inhibing the coalescence and the mixture obtained is introduced in the lower part of an essentially obstacle-free reactor wherein an almost complete reaction takes place between the oxygen and the hydroquinone present in the hydrogenated solution. The device for implementing said method comprises a mixer (1), a reactor (6) with a cleared bottom part and, if required, a distributor (7).
机译:为了执行通过使用蒽醌法生产过氧化氢的氧化封闭回路,根据该方法,氧化剂气体在低于100℃的温度下在平行流反应器中在氢化溶液中通过。在低于15 bar的压力下并通过提高氧化步骤中的反应速度,在氢化步骤之后,将氢化溶液与氧化剂气体充分混合,形成抑制聚结的体系,并将所得混合物引入到反应釜的下部。基本上无障碍的反应器,其中氧气和氢化溶液中存在的氢醌之间几乎完成了反应。用于实施所述方法的装置包括混合器(1),具有澄清底部的反应器(6),以及如果需要的话是分配器(7)。

著录项

  • 公开/公告号AR240549A1

    专利类型

  • 公开/公告日1990-05-31

    原文格式PDF

  • 申请/专利权人 OESTERREICHISCHE CHEMISCHE WERKE GES.M.B.H.;

    申请/专利号AR19860303866

  • 发明设计人

    申请日1986-05-06

  • 分类号C01B15/02;

  • 国家 AR

  • 入库时间 2022-08-22 06:20:04

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