Aqueous effluent solutions containing metal cations may be treated with an extractant comprising an organophosphinic acid, a di-2- ethylhexyl phosphoric acid and/or an aliphatic amine to selectively separate chromium, nickel, cobalt, copper and lead cations from the aqueous solution. Typical extraction techniques include liquid-liquid extraction employing either mixer settlers or columns, liquid membrane extraction and selective supported membrane extraction.
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