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SPECIMEN HOLDER FOR INFRARED EMISSION SPECTROSCOPY

机译:红外发射光谱专用标本架

摘要

PURPOSE:To measure an infrared emission spectrum of a thin film specimen with good accuracy and sensitivity by thermally isolating a specimen holder from the heated specimen and allowing infrared emission from the specimen surface to pass through while other infrared emission from a specimen substrate, a substrate side wall or a heater is shielded. CONSTITUTION:A this film specimen 1 of a substrate is pushed by a heater 2 and a specimen holder 3 from backward to be adhered and fixed to them. Infrared emission having a maximum of radiation intensity in a direction approximately parallel to a surface of the specimen and having polarization characteristics deflected in a direction perpendicular to the specimen surface is radiated from the surface of the specimen 1 which has been heated by the heater 2. At this time infrared emission is radiated also from the surfaces of the holder 3 and the heater 2. The infrared emission can be thermally isolated from the holder 3 by a spacer as well as isolated by a specimen holder cover 4 equipped with an aperture which allows the infrared emission only from the specimen surface to pass through. In addition the surface of the holder cover 4 is finished in a mat with unevenness so that a surface area in parallel with the thin film surface can be remarkably reduced.
机译:目的:通过将样品架与加热的样品热隔离,并允许样品表面的红外辐射通过,而其他样品衬底的红外辐射通过,从而以良好的精度和灵敏度来测量薄膜样品的红外光谱。侧壁或加热器被屏蔽。组成:该基板的薄膜样本1被加热器2和样本支架3从后方推动,以粘附并固定到它们上。从已经被加热器2加热的样本1的表面辐射出在大致平行于样本表面的方向上具有最大辐射强度并且在垂直于样本表面的方向上偏转的偏振特性的红外发射。此时,红外辐射也从支架3和加热器2的表面辐射。红外辐射可以通过垫片与支架3热隔离,也可以通过带有孔的样品支架盖4隔离。红外辐射仅从样品表面通过。另外,保持器盖4的表面被加工成具有凹凸的垫子,从而可以显着减小与薄膜表面平行的表面积。

著录项

  • 公开/公告号JPH03235038A

    专利类型

  • 公开/公告日1991-10-21

    原文格式PDF

  • 申请/专利权人 HITACHI LTD;

    申请/专利号JP19900029617

  • 发明设计人 TOCHIGI KENJI;MOMOSE HIDETO;

    申请日1990-02-13

  • 分类号G01J3/443;G01N21/01;G01N21/21;G01N21/35;G01N21/3563;

  • 国家 JP

  • 入库时间 2022-08-22 06:05:14

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