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A process for the preparation of a higher concentrated hydrochloric acid from a hydrochloric acid with a concentration which is located below the azeotropic concentration

机译:由浓度低于共沸浓度的盐酸制备高浓度盐酸的方法

摘要

in a process for the production of a more concentrated hydrochloric acid in a hydrochloric acid with a below the azeotropen concentration the concentrationin particular, the washing fluid from a washing at least a hcl containing exhaust gas, especially exhaust gas of an incinerator.is the production of high concentrated acid in a simple manner and in eradication of hcl in liquid phase forthat the ausgangssu00e4ure (1) in a first stage (2) with energy intake (3; 5) water (5) is expelled.in a second stage (4) with a circuit (k1) of high boiling temperature heated aqueous solution of water and hcl is expelled and the steam exhaust (3) of the second stage (4) of the firststage as heizdampf is supplied.that the first stage (2), draining aufkonzentrierte hydrochloric acid (9) and the circuit (k1) of the second stage (4) for draining calciumchloridhaltige solution (14) and (15), and a third stufe (17) with a cycle (k2) is fed, in the intake of heat (20) hcl and water be exorcised.and that the exhaust gas (21) of the third stage (17) of a condensation (22) for the removal of water and then a absorptionsstufe (24) is supplied.in the intake of water (25) the higher concentrated produktsalzsu00e4ure (26) is generated.with solution (29) from the circuit (k2) of the third stage (17) in the circuit (k1) of the second stage (4) is reduced, and...
机译:在生产低于浓共沸物浓度的盐酸中的更浓盐酸的方法中,该浓度尤其是来自洗涤至少含HCl的废气,尤其是焚烧炉废气的洗涤液。以简单的方式清除液相中的浓盐酸,因为在第一阶段(2)的能量吸收(3; 5)中的水(5)在第二阶段被排出。 (4)用高沸点加热的水和氯化氢的水溶液的回路(k1)排出,并以heizdampf的形式供应第一级的第二级(4)的蒸汽排出口(3)。 ),排空盐酸三苯甲酸酯(9)和第二阶段(4)的回路(k1),用于排泄氯代卤化钙溶液(14)和(15),并送入带循环(k2)的第三瓶(17),吸入热量(20)盐酸和水后,冷凝物(22)的第三阶段(17)的废气(21)用于除水,然后提供吸收剂(24)。在水(25)的入口中,较高浓度的产品(26)用第二级(4)的电路(k1)中第三级(17)的电路(k2)的溶液(29)还原,...

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