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PROCESS FOR MANUFACTURING RARE EARTH OXIDE CERAMIC SCINTILLATOR BY USING OXALATE PRECIPITATE DISPERSED WITH AMMONIUM

机译:用分散有草酸铵的草酸盐沉淀法制备稀土氧化物陶瓷闪烁体的方法

摘要

A method of forming polycrystalline rare earth oxide ceramic scintillators formed by dissolving a mixture of oxides of the scintillator in an aqueous hydrochloric or nitric acid solution to form a rare earth solution, precipitating oxalates from the rare earth solution, calcining the oxalates to form the respective oxides, cold pressing the oxides to form a compact, and sintering the compact in a reducing atmosphere or vacuum to form the scintillator, the method being improved by precipitating the oxalates by admixing the rare earth solution with an oxalic solution comprised of, oxalic acid and ammonium ions in an amount that disperses the oxalate precipitates.
机译:一种形成多晶稀土氧化物陶瓷闪烁体的方法,该闪烁体是通过将闪烁体的氧化物的混合物溶解在盐酸或硝酸水溶液中形成稀土溶液,从稀土溶液中沉淀草酸盐,煅烧草酸盐而形成的。氧化物,冷压氧化物以形成压块,然后在还原性气氛或真空中烧结该压块以形成闪烁体,该方法通过将稀土溶液与草酸和草酸混合而沉淀出草酸盐而得到改进。铵离子的分散草酸盐沉淀量。

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