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Sample setting method and apparatus for flame type atomic absorption spectrophotometry

机译:火焰型原子吸收分光光度法的样品设置方法及装置

摘要

There are disclosed a method for setting a sample for flame type atomic absorption spectrophotometry by a method called microsampling method and an apparatus therefor.;An atomizer (16) has connected thereto via tube (14) a sample receiver (12) for micro-sampling. The sample receiver (12) has its funnel-shaped upward opening and has connected the tube (14) to the base of the funnel. A control unit (66) controls to make sure that the sample injected into the sample receiver will be so positioned in the tube (14) that a solvent is nearer to the vaporizer than the sample, preferably the solvent is also present nearer to the side of the sample receiver (12) than the sample.;The presence of solvent in the tube (14) nearer to the vaporizer (16) than the sample delays the sample being sucked by the vaporizer (16), this preventing interruption of the sample flow in the tube (14) and helping make the atomic absorption waveform more stable.
机译:公开了一种通过称为微量取样法的方法将样品放置在火焰型原子吸收分光光度法中的方法及其设备。雾化器(16)经由管(14)连接至其用于微量取样的样品接收器(12)。 。样品接收器(12)具有其漏斗形的向上开口,并将管子(14)连接到漏斗的底部。控制单元(66)进行控制以确保注入到样品接收器中的样品将放置在管(14)中,使得溶剂比样品更靠近蒸发器,优选地,溶剂也更靠近侧面存在。样品接收器(12)的体积比样品的体积小;在比样品更接近蒸发器(16)的管(14)中存在溶剂会延迟样品被蒸发器(16)吸入,从而防止样品中断气体在管(14)中流动,并有助于使原子吸收波形更稳定。

著录项

  • 公开/公告号EP0514678A1

    专利类型

  • 公开/公告日1992-11-25

    原文格式PDF

  • 申请/专利权人 SHIMADZU CORPORATION;

    申请/专利号EP19920106938

  • 发明设计人 KOJIMA SEIJI;SASAKI KIKUO;HONDA AKIRA;

    申请日1992-04-23

  • 分类号G01N21/72;G01N1/10;

  • 国家 EP

  • 入库时间 2022-08-22 05:06:54

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