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Coupling capillary gas chromatography to traditional liquid chromatography detectors

机译:将毛细管气相色谱仪与传统液相色谱仪联用

摘要

Apparatus and methods are provided for using a detector designed for use with liquids to detect resolved analytes in an effluent stream from a gas chromatography instrument. The gaseous stream is entrained by a flowing liquid solvent, and at least a portion of the analytes are transferred from the gas phase to the liquid phase. The liquid solvent containing the analytes is then conveyed to a detector designed for liquid analysis. Thus, the present invention gives the analyst more options for detecting an analyte or a group of analytes, thereby providing greater flexibility in optimizing the sensitivity or selectivity of the analysis. Furthermore, the present invention allows gaseous effluents to be analyzed by detectors which more readily permit sample recovery than the detectors currently being used to analyze gaseous effluents.
机译:提供了用于使用设计成与液体一起使用的检测器的设备和方法,以检测来自气相色谱仪的流出物流中的分解的分析物。气流被流动的液体溶剂夹带,并且至少一部分分析物从气相转移到液相。然后将包含分析物的液体溶剂输送到设计用于液体分析的检测器中。因此,本发明为分析人员提供了用于检测分析物或一组分析物的更多选择,从而在优化分析的灵敏度或选择性方面提供了更大的灵活性。此外,本发明允许通过检测器分析气态流出物,该检测器比当前用于分析气态流出物的检测器更容易允许样品回收。

著录项

  • 公开/公告号US5242471A

    专利类型

  • 公开/公告日1993-09-07

    原文格式PDF

  • 申请/专利权人 THE DOW CHEMICAL COMPANY;

    申请/专利号US19920887996

  • 发明设计人 PATRICK W. LANGVARDT;DAN A. MARKHAM;

    申请日1992-05-22

  • 分类号B01D15/08;

  • 国家 US

  • 入库时间 2022-08-22 04:57:48

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