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Dynamic shear rheometer and method

机译:动态剪切流变仪和方法

摘要

An improvement in a rheometer and the method for measuring rheological properties of a viscoelastic test specimen at different temperatures, at which different temperatures the viscoelastic properties exhibit a relatively wide difference, wherein the test specimen is placed between and is coupled with opposed plates, one of the opposed plates is oscillated angularly relative the other of the opposed plates, and the angular displacement of one of the plates relative to the other of the plates and the torque associated with the relative angular displacement are measured within a predetermined optimum range of torque and angular displacement for determining the rheological properties, couples a first contact surface on one of the opposed plates with the test specimen to establish a first contact area between the one of the opposed plates and the test specimen when the test specimen is at one of the different temperatures, and couples a second contact surface on the one of the opposed plates with the test specimen to establish a second contact area between the one of the opposed plates and the test specimen when the test specimen is at another of the different temperatures, the first contact area being different in area from the second contact area such that, by virtue of the difference in area between the first and second contact areas, the torque and the relative angular displacement measured at each of the one and the another of the different temperatures fall within the predetermined optimum range.
机译:流变仪的改进和用于在不同温度下测量粘弹性测试样品的流变特性的方法,在不同温度下,粘弹性特性表现出相对较大的差异,其中将测试样品放置在相对的板之间并与之相对联,其中之一是相对的板相对于另一个相对的板以角度振荡,并且在扭矩和角度的预定最佳范围内测量其中一个板相对于另一个板的角位移以及与相对角位移相关的扭矩。用于确定流变性质的位移,将其中一个相对板的第一接触表面与试样耦合,以便在试样处于不同温度之一时在相对板之一和试样之间建立第一接触面积,并在相对的平板之一上耦合第二接触面当测试样品处于另一不同温度时,与测试样品建立相对的板之一与测试样品之间的第二接触面积,第一接触面积与第二接触面积不同,从而,由于第一和第二接触区域之间的面积差,在不同温度的一个和另一个上分别测得的转矩和相对角位移落在预定的最佳范围内。

著录项

  • 公开/公告号US5271266A

    专利类型

  • 公开/公告日1993-12-21

    原文格式PDF

  • 申请/专利权人 RHEOMETRICS INC.;

    申请/专利号US19910803948

  • 发明设计人 ALAN R. ESCHBACH;

    申请日1991-12-06

  • 分类号G01N11/02;

  • 国家 US

  • 入库时间 2022-08-22 04:32:30

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