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Process for measurement of the degree of cure and percent resin of glass- fiber reinforced epoxy resin prepreg

机译:玻璃纤维增​​强环氧树脂预浸料的固化度和树脂百分率的测量方法

摘要

The degree of cure and the amount of epoxy resin in a glass fiber reinforced epoxy resin prepreg is measured by exposing the prepreg to a series of light pulses created by optical filters transmitting light at predetermined bandwidths about selected wavelengths, preferably centered at wavenumbers of about 4529 cm.sup.-1 and 4055 cm.sup.-1 and measuring the amount of epoxy groups and methyl groups present relative to reference values from the electrical pulses produced by a phase sensitive photoelectric detector disposed to receive said light pulses after being exposed to said prepreg. When such measurements are made in a continuously moving sheet of prepreg, it is possible to control the variation of percent cure and resin content to no greater than .+-.3% cure and .+-.3% resin content over a distance of at least 400 yds (366 m).
机译:玻璃纤维增​​强的环氧树脂预浸料中的固化程度和环氧树脂的量是通过将预浸料暴露于由光学滤光片产生的一系列光脉冲来测量的,这些滤光片以大约选定波长的预定带宽传输光,优选以大约4529的波数为中心cm.sup.-1和4055 cm.sup.-1,并从相敏光电探测器产生的电脉冲测量相对于参考值存在的环氧基和甲基的数量,该相敏光电探测器被设置为在曝光后接收所述光脉冲预浸料说。当在连续移动的预浸料片中进行此类测量时,可以将固化百分比和树脂含量的变化控制在不超过+/- 0.3%的固化范围和+/- 0.3%的树脂含量的范围内。至少400码(366 m)。

著录项

  • 公开/公告号US5457319A

    专利类型

  • 公开/公告日1995-10-10

    原文格式PDF

  • 申请/专利权人 ALLIEDSIGNAL INC.;

    申请/专利号US19940239072

  • 发明设计人 AMY L. MOE;JIRI D. KONICEK;

    申请日1994-05-06

  • 分类号G01N21/35;

  • 国家 US

  • 入库时间 2022-08-22 04:04:15

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